App ID: FLM-C220009
Comixsil HAX直接分析草甘膦的柱效，峰形和保留時(shí)間研究
Column: Comixsil HAX 3u 100*2.1mm (P/N: FMD-HAX3-BONU)
Mobile phase: A: Water, B: ACN, C: 100 mM AmFm pH 3
Methods: (according to the table)
Flow rate: 0.25 ml/min
Detection: CAD, Range 50, Filter high, offset 15%
Sample: 1 mg/ml
Injection: 3 uL
|
N |
Method Description |
A, % |
B, % |
C, % |
Symmetry |
Plate Count |
|
1 |
60% ACN with 20 mM AmFm pH 3 |
60 |
30 |
20 |
0.98 |
1376 |
|
2 |
60% ACN with 10 mM AmFm pH 3 |
60 |
35 |
10 |
1.42 |
1358 |
|
3 |
40% ACN with 10 mM AmFm pH 3 |
40 |
50 |
10 |
1.25 |
1635 |
|
4 |
20% ACN with 10 mM AmFm pH 3 |
20 |
70 |
10 |
1.09 |
2271 |
|
5 |
20% ACN with 20 mM AmFm pH 3 |
60 |
20 |
20 |
0.86 |
1835 |
一般的非質(zhì)譜常規(guī)含量分析，建議采用 Comixsil HAX 3u 100*4.6mm或 150*4.6mm
